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Beilstein J. Org. Chem. 2015, 11, 957–965, doi:10.3762/bjoc.11.107
Graphical Abstract
Scheme 1: Redox-induced conformational switching of diphenyl-TTFV 1.
Scheme 2: Synthesis of carboxylated TTFV 6 and DTF 7.
Scheme 3: Complexation of compounds 6 and 7 with Zn(II) ions.
Figure 1: UV–vis spectra of TTFVs 5 and 6 (solid lines) and DTF 4 and 7 (dashed lines). Compounds 4 and 5 wer...
Figure 2: Cyclic voltammograms of compounds 4–9. Experimental conditions: supporting electrolyte: Bu4NBF4 (0....
Figure 3: FTIR spectra of compounds 6–9.
Figure 4: PXRD patterns of the Zn-TTFV coordination polymer 8 (red line) in comparison with the diffraction d...
Figure 5: (A) Nitrogen adsorption isotherm of coordination polymer 8 measured at 77 K. Inset: pore size distr...
Figure 6: DSC traces of compounds 6–9 measured under a nitrogen atmosphere. Scan range: 25–400 °C, scan rate:...